Can You Remove Thc From CBD Oil

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Extract the full spectrum of CBD When prioritising the best CBD products, it’s important that each step of the process is carried out with care and precision. You can grow high-quality hemp, with a large percentage of cannabidiol (CBD), but all of that goes to waste without the proper extraction techniques. So, that ra How to extract CBD oil – The extraction process & how to make CBD oil CBD (Cannabidiol) is a compound that has shown promise in a variety of medical applications, like relief from pain and THC Removal – Remove THC from CBD | B/R Instrument Blog | Industry Leader in Laboratory Distillation Equipment

Which CBD oil extraction method is the best?

When prioritising the best CBD products, it’s important that each step of the process is carried out with care and precision. You can grow high-quality hemp, with a large percentage of cannabidiol (CBD), but all of that goes to waste without the proper extraction techniques. So, that raises the question: which method is best?

At Vitality CBD we often discuss the importance of choosing a quality CBD oils, and how premium extraction techniques contribute to a better product. To truly understand why high-end extraction methods matter, let’s first explore how CBD is synthesised.

What is CBD?

CBD, or cannabidiol, is one of over a hundred different cannabinoids found in plants from the Cannabis family. The most famous of these cannabinoids, tetrahydrocannabinol, or THC, is the one that induces the “stoned” effects typically associated with recreational Cannabis use. On the other hand, studies have repeatedly shown that CBD does not get you high.

Currently we know that when introduced to your body, CBD interacts with your pre-existing endocannabinoid system. Understanding that the human body already generates cannabinoids that bear a great similarity to CBD in structure and function is step one in understanding why CBD oil is proving so popular.

Cannabidiol is actually synthesised in the trichomes of the female hemp plant, alongside the other cannabinoids, terpenes, and flavonoids. The need to create CBD oils that retain CBD and other cannabinoids whilst removing the THC is part of why extraction techniques are so important.

How do you extract CBD?

When we extract the best CBD, the end goal is to harvest it in a concentrated form so that it can then be mixed into CDD e-liquids, CBD oils and CBD topicals. That’s why we use a strain of hemp called Cannabis sativa L., renowned for its high CBD levels.

As we’ve mentioned, CBD is actually a constituent in a vast sea of hemp compounds, so extraction isn’t as easy as it first may seem. However, all of these techniques were first developed for other purposes, like extracting essential oils from flowers.

At Vitality CBD we use two different techniques specifically (typically in conjunction) but we’ll discuss all the options available, and how they affect the end result. As always, if you have any further questions drop us an email on our contact page.

CO2 extractions of cannabidiol

The most expensive and most popular CBD extraction method (particularly amongst manufacturers offering a premium product) involves using CO2. This is because it provides a clean, precise extraction that massively reduces the contamination potential of other methods.

The applications of CO2 extractions stem far beyond just hemp products. CO2 extractions are used to decaffeinate coffee beans, to extract the nicotine from loose-leaf tobacco, and to precisely extract spices and flavours.

CO2 extractions can be split into supercritical and subcritical categories (there’s also ‘mid-critical’, a halfway point between the two), but supercritical is the most common, and the one we use at Vitality CBD for all of our CBD products. We’ll breakdown the differences between each below.

The shared methodology between the two essentially entails running pressurised carbon dioxide across the hemp plant to strip away the desired phytochemicals (literally: plant chemicals). When treated to certain conditions, CO2 actually acts like a solvent, without any of the potential side-effects.

Supercritical CBD extraction

Starting with the liquid form of CO2, a supercritical method involves increasing the temperature and pressure of the CO2 until it becomes ‘supercritical’. This means that the CO2 has properties of both gas and liquid: it is able to fill a container like a gas, whilst also having the density of a liquid.

In this supercritical state, CO2 acts as a solvent when applied to the hemp plant without denaturing any of the compounds. The need to maintain the right pressure and temperature explains why CO2 extractions use expensive equipment, resulting in the best CBD.

Once the supercritical CO2 has been passed through the hemp extract, the resultant solution is passed into a separator to be (you guessed it) separated. The CO2 is stored to be used again, whilst the desired hemp compounds are removed and taken to the next step in the process.

Subcritical CBD extraction

The immediate distinction with a subcritical hemp extraction is the lower temperature and lower pressure. As a result, the process takes longer, but it also further reduces the chances of denaturing the more delicate compounds, like terpenes.

Whilst the yield is smaller than with supercritical, it also allows for lighter oils and other sensitive compounds that might otherwise be dismantled in the process to be extracted. However, the trade off is that heavier, more resinous material will typically get left behind.

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Solvent CBD extractions

Probably the cheapest and easiest of all the methods available (you could easily do it at home without buying any specialist equipment. not that we recommend this), solvent extractions are also generally considered to be the most likely to cause issues with the end product.

A solvent extraction involves running the solvent in question—typically either butane or ethanol—to the hemp plant matter. This strips the cannabinoids into the liquid, which is then evaporated so as to leave behind a concentrated oily residue with the hemp compounds in.

The main problem is that the solvent not only removes the cannabinoids, terpenes and flavonoids, but also inadvertently extracts chlorophyll. This occasionally leads to unwanted side effects, and will cause the taste to become much more bitter.

Likewise, the compounds that the solvent does remove can either be denatured, or just degraded entirely during the extraction process. As such, whilst it’s the cheapest and easiest method to do on a mass scale, there’s a reason why many companies are phasing it out. When you buy CBD with us, you can be confident it’s not been treated this way.

Olive oil CBD extraction

An olive oil extraction is most commonly done by home brew enthusiasts looking to create their own CBD oils. Though near any oil can be used in this process, olive oil is preferred due to its masking flavour and versatility.

The first step is to either grind the hemp very finely, or to decarboxylate it, a complex word which here means: heat it at a certain temperature. Through this process, several of the cannabinoids have their chemical make-up converted, making some more potent and others easier to extract.

After the initial heating, you then heat the hemp matter further in the olive oil, a process by which the compounds are extracted to the oil. Whilst this is perfect for home users, it results in a low yield and a highly perishable product that isn’t practical on a mass scale.

Dry ice CBD extraction

Whilst the name alone suggests high-tech scientific experimentation, this is another method that can be performed at home (assuming you have access to dry ice). It also benefits from the lack of denaturing solvents, resulting in a cleaner and purer end product.

The process involves flash-freezing the loosely chopped hemp extract, and then sieving the frozen trichomes through a mesh bag. These in turn can then be used as the basis for your cannabidiol oil—it’s really that simple.

Since this is a relatively haphazard and difficult to measure method, the quality is not always ensured depending on how well the hemp is frozen and how vigorously it is sieved. However, if you can get safe access to dry-ice this is a clean alternative to solvents for creating your own CBD oil.

Which CBD extraction method is best?

At Vitality CBD, we would recommend either of the two mentioned CO2 extraction techniques, depending on what compounds you want to prioritise extracting. All of the others have their uses, of course, but CO2 is the best all-rounder.

Learn more about CBD

As mentioned earlier, grasping why a clean and accurate extraction is important is premised on understanding just what is being extracted. Read on here for our supporting articles on terpenes and flavonoids.

If you’ve got any further questions about CBD extraction techniques, or some information you’d like to share with us, our experienced team are always on hand to field any questions. You can reach our friendly team via our contact page, or alternative you can go check out our full CBD range here!

You may have seen full spectrum CBD, broad spectrum CBD and pure CBD when you have been looking at CBD. So what do these common pieces of terminology mean?

In a comprehensive survey on the current state of the UK CBD marketplace, the Centre for Medicinal Cannabis has revealed some remarkably high user figures across the board.

Find out more about cannabidiol, more commonly known as CBD. Discover the uses and history of these incredibly popular new wellness ingredient.

How to extract CBD oil – The extraction process & how to make CBD oil

CBD (Cannabidiol) is a compound that has shown promise in a variety of medical applications, like relief from pain and anxiety which are most common, along with many other ailments. A major benefit to CBD is that it doesn’t contain THC, which is the compound that makes users high, so this makes CBD an ideal product for children. Below you will find a step by step outline of how cbd oil is made.

CBD extract oil from cannabis or hemp.

There are many ways to extract the oil from the plant and make cbd oil. Apeks CO2 extraction systems use CO2 as a solvent to extract the oil. The solvent is considered a cleaner, purer form of extraction because there is no residue after extraction.

To isolate the individual compounds (CBD being one of them), the extracted oil needs to be distilled after extraction. The first step is a process called Winterization, followed by Short Path Distillation.

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Winterization

Winterization is the process to remove undesirable elements that were extracted from the plant, for example fats, waxes, and lipids. This process is only needed when the oil was extracted at high pressure/high temperature (supercritical) because this intense extraction pulls everything from the plant, including material you don’t want in the final products. The extracted oil is effectively crude oil, which needs refining.

Once extracted, the mixture is combined with 200 proof alcohol and stirred vigorously until completely mixed. It’s then placed in a deep freezer overnight. In the morning, the mixture looks cloudy and is ready for filtration. One way to filter out the fats, etc. is to run it through a filter paper into an extraction jar. A common piece of equipment for this is a Buchner Funnel. Once it’s been filtered to satisfaction and the undesirable elements have been removed, it’s time to remove the alcohol. This is done using heat. The extraction is warmed and as its warmed, the alcohol evaporates since the boiling point of alcohol is lower than the oil. The removed alcohol may then be used on a different batch of crude oil.

Mixing oil and alcohol prior to freezing

Short Path Distillation equipment

Short Path Distillation

To further refine the CBD extract, and to isolate the CBD, the oil goes through Short Path Distillation. This works in much the same way as Winterization in that the extract is heated and each compound is then separated because each one has a different boiling point. In this way, each compound is isolated and can be used by itself.

Benefits and Uses of CBD

Research is showing that CBD extract has a huge potential in the medical market. CBD’s common benefits are treating anxiety, reducing pain and inflammation, helping prevent seizures, among many others. Because it’s a natural extract, there are few, if any, side effects. The extract works with the body’s endocannabinoid system, which is the system’s method of regulating processes, like pain, mood, appetite, and memory. CBD works with the natural system rather than being an unnatural substance, so the body doesn’t try to reject it. CBD extract may be sourced from cannabis or hemp, most typically from hemp, which is naturally high in CBD. Cannabis can also be bred to have low THC levels and high CBD levels, but it’s possible that the THC will get concentrated and included in your final products.

Tne Entourage Effect

Despite the benefits of CBD as an isolate, there is much to be said for treating patients with all the compounds in the plant, not as separate isolates. Patients can still use the oil without getting high, as long as the THCa has not been heated, which converts it into THC, which is what makes you high. The Entourage Effect is the effect that all the compounds of the plant have on the body, as a whole.

Hemp and cannabis oil extraction processes and techniques.

Andy is on a panel of experts, answering questions from the community. We compiled a collection of questions and answers below, about hemp and cannabis oil extraction processes and techniques.

Click here to get more information on the CBD Extraction Process.

What are the safest and most effective ways to extract and produce CBD-rich cannabis oil? CO2, oil, or ethanol?

Question:
What are the safest and the most effective ways to extract and produce CBD oil? CO2, oil, or ethanol?

Answer:
Thanks for the great question! There are really 2 questions here, so I’ll try to answer them separately.

First question: What are the safest ways to extract? When it comes to extraction, safety is an important issue and has many areas to consider. The list below represents some of the major areas that need to be addressed with the popular solvents being used in the cannabis industry today:

  • Materials of Construction- Stainless steel materials for food/consumed oil applications
  • Electrical for Flammable Solvents – Class 1, Division 1 (explosion proof) electrical components for compressed flammable gasses, Class 1, Division 2 for ethanol/alcohol
  • Electrical, Non Flammable Solvents – NEMA 4x wash down electrical enclosures
  • Pressure Rating – usually 300 psi for hydrocarbons, 2000 or 5000psi for CO2.
  • Overpressure Protection – non-isolable relief valves set to 110% of maximum allowable working pressure
  • Food grade – welds in contact with extracted material should be ground flush and polished
  • Accessibility for Cleaning – vessels and piping should be accessible from both ends to allow proper cleaning
  • Storage tanks – should be stainless steel to prevent corrosion

Facility – In addition to the equipment considerations, the facility must also be appropriate for the extraction solvent.

  • Compressed Flammable Gasses – Class 1, Division 1 facility. This includes electrical fixtures, and also monitoring and evacuation equipment in the event there is a release of flammable gas into the area around the equipment.
  • Ethanol/Alcohol – vent hood or equivalent walk in vent area
  • CO2 – asphyxiation hazard. Monitoring and audible alarm to warn of leaks.
  • CO2 – Generally Regarded as Safe (GRAS) by the FDA for consumption
  • Compressed gas – GRAS for use as a propellant, states differ on safe residual solvent levels
  • Ethanol – GRAS for food products, states differ on safe residual solvent levels
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So the answer to the question about safety really doesn’t have anything to do with the solvent, rather the equipment chosen and the facility where the extraction is performed determine safety. The solvents commonly used in extractions today all have pros and cons, and all can be operated safely as long as proper guidelines and regulations are followed.

I addressed the safety question in the first part of the answer, in the second part I’ll address the efficiency question: What is the most effective way to extract CBD-rich oil?

A major problem facing the cannabis industry today is a lack of commonly accepted standards – as evidenced by the question referring to “CBD-rich”. Does “CBD-rich” mean 40% CBD? 99% CBD? And CBD in what form, CBD, CBD-A or some combination? There are groups that are working towards creating standards, such as FOCUS and ASTM, but they have not been widely accepted yet. Without standards, quality also becomes difficult to determine because the only standard is personal subjectivity.

That being said, there are some generalizations about extraction methods that can be made. Keep in mind – every extraction method has benefits and drawbacks. Each method will shine in certain applications, and perform poorly in other. No method is great at everything.

THC Removal – Remove THC from CBD

Consumers are attracted to the purported health benefits of CBD but understand that THC naturally occurs in hemp along with other minor cannabinoids. They do not want to consume THC because they don’t want the “high” the comes along with THC or they don’t want to possibly test positive for THC in a work drug screening. The good news is that THC can be separated from CBD so that it can be consumed without concern for unwanted THC.

There are several ways to remove THC from CBD oil, CBD extracts and CBD distillate. The products can be THC Free (T Free) or low THC (0.3% or lower) which does not produce a “high”.

Broad Spectrum CBD

Broad spectrum products contain all of the cannabinoids with little THC (less than 0.3%/wt). This should not to be confused with THC Free or T-Free oil which contains no THC.

Chromatographic methods such as flash chromatography and CPC use solvents and a stationary phase to fractionate the cannabinoids from one another. In these processes, the THC is isolated and removed from the other cannabinoids. But, there is the unwanted side effect of losing some or all of the minor cannabinoids and CBD in the THC fraction.

In addition to using large volumes of solvents, chromatographic methods remove THC at a fairly slow rate and some CBD is lost in the process. At the same time, it requires an experienced operator to be available at all times during operation.

SCB-15 THC Remediation System

SCB-15 – Solvent Free THC Remediation System

Another technique for removing THC from full spectrum CBD is the SBC solvent free remediation system. This THC removal process is solvent free. It uses automation to maintain the optimum vacuum, temperature, and other parameters to remove THC (and some CBD) from the CBD oil. An operator occasionally monitors the THC level by Near Infrared or HPLC. Up to 100 liters of CBD or CBG oil can be remediated in 12-24 hours.

Pure CBD

Pure CBD (also called isolate) can be produced by crystallizing CBD oil/extract/distillate. CBD oil is mixed with pentane and cooled until the CBD crystallizes (crashes out). Crystallized CBD is filtered, rinsed, and dried. Purities of 99+% are possible. Re-crystallization can increase the purity even higher. All THC is removed along with minor cannabinoids.

CBD Crystals or “Isolate”

Full spectrum CBD

The “entourage effect” is the name given to the synergistic benefits of cannabinoids and terpenes working together in your body. It has been the subject of study for many years, however we are still only beginning to understand some of the possibilities. The entourage effect can produce many different results depending on the combinations.

Full spectrum is a term that applies to extracts or oils that contain all of the naturally occurring cannabinoids from the plant. For hemp products this often includes more than 0.3% THC. In order to stay legally compliant, something must remove the THC.

4 Comments

this is what i want to start doing as my income resource i want to learn everything i can about how this is done and if i need to attend a class or school to get the right training if you would please send me some information on what i should be doing in order to start the process would really be great thanks very much for your time ———————————- scott

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